Carry out auto tuning using the ESI unit/IonFocus Unit to perform sensitivity adjustment, resolution adjustment, and mas

A detector voltage of about -1.6 to -3.0 kV is normal. The detector deteriorates and the detector voltage increases at

For some compounds, probe position may give a great influence to sensitivity. If the probe position is out of place, sen

The following causes are possible. 1. The wrong standard sample was used. Click here for Standard Sample info

You can adjust the spray position by turning the position adjustment knob. To adjust the spray position, first press th

«Main Cause» 1. There is a gas leak. 2. The gas is not flowing. «Countermeasure» 1. Check the gas tubing

Turbo molecular pumps require maintenance every 25,000 hours (about 3 years). Contact a Shimadzu sales or service rep

1. Turning the Power ON a) Turn ON the power to each of the LC and MS units. The POWER indication lamp on the fron

Check if the DL, heater flange, and ionization unit are mounted properly. Click here for replacing the DL. If the pr

It is set to turn on cooperation Nebulizing Gas and Pump. The [Gas Control Mode] tab page is located in the [Setting

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Auto Tuning (LCMS)

Carry out auto tuning using the ESI unit/IonFocus Unit to perform sensitivity adjustment, resolution adjustment, and mass calibration of the instrument. Per... Show Detail
- No：3294
- Date of Issue：2020/11/18 15:33
- Category： Maintenance
- Brached FAQ
Interpreting tuning results (LCMS)

A detector voltage of about -1.6 to -3.0 kV is normal. The detector deteriorates and the detector voltage increases at a rate that depends on its conditions... Show Detail
- No：3299
- Date of Issue：2020/11/18 15:33
- Category： Setting
- Brached FAQ
How to check for ESI Probe position problems (LCMS)

For some compounds, probe position may give a great influence to sensitivity. If the probe position is out of place, sensitivity fluctuation may become large... Show Detail
- No：3314
- Date of Issue：2020/11/19 12:47
- Category： Troubleshooting
Auto tuning has failed (LCMS)

The following causes are possible. 1. The wrong standard sample was used. Click here for Standard Sample information. 2. The standard sampl... Show Detail
- No：3301
- Date of Issue：2020/11/26 13:54
- Category： Troubleshooting
ESI/DUIS spray position adjustment (LCMS)

You can adjust the spray position by turning the position adjustment knob. To adjust the spray position, first press the adjustment knob so that it pops out... Show Detail
- No：3300
- Date of Issue：2020/11/26 14:56
- Category： Setting
- Brached FAQ
The gas is not flowing according to the specified value (...

«Main Cause» 1. There is a gas leak. 2. The gas is not flowing. «Countermeasure» 1. Check the gas tubing. As a start-of-work inspection, ... Show Detail
- No：3302
- Date of Issue：2020/11/30 13:09
- Category： Troubleshooting
Error [Turbo molecular pump should be overhauled.] (LCMS)

Turbo molecular pumps require maintenance every 25,000 hours (about 3 years). Contact a Shimadzu sales or service representative. Show Detail
- No：3303
- Date of Issue：2020/11/30 13:31
- Category： Troubleshooting
LCMS Starting the Instrument

1. Turning the Power ON a) Turn ON the power to each of the LC and MS units. The POWER indication lamp on the front of the instrument will light in gre... Show Detail
- No：4501
- Date of Issue：2020/12/09 16:28
- Last Updated：2022/06/20 10:26
- Category： Setting
- Brached FAQ
The temperature of the DL, heated block or interface heat...

Check if the DL, heater flange, and ionization unit are mounted properly. Click here for replacing the DL. If the problem persists, contact a Shimadzu sa... Show Detail
- No：4741
- Date of Issue：2021/01/08 11:24
- Category： Troubleshooting
LC pump cannot solvent delivery (LCMS)

It is set to turn on cooperation Nebulizing Gas and Pump. The [Gas Control Mode] tab page is located in the [Setting Options] sub-window. To open this sub... Show Detail
- No：4743
- Date of Issue：2021/01/08 13:58
- Category： Troubleshooting

31-40 of Total 133

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