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(GCMS) Chemical Ionization(CI, NCI) Excessive Introduction of Reagent Gas
(GCMS) Chemical Ionization(CI, NCI) Excessive Introduction of Reagent Gas
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Answer
Sometimes too much reagent gas is introduced during reagent gas adjustment. If this happens, extract excess reagent gas by following the procedure below.
1. Close the pressure-regulating valve of the pressure regulator slightly.
2. Click the [Reagent Gas] button on the [Instrument Control] bar to close the valve.
As a result, the valve of the reagent gas control unit is closed, and reagent gas in the analysis tube is extracted from the controller by the rotary pump.
As a result, the valve of the reagent gas control unit is closed, and reagent gas in the analysis tube is extracted from the controller by the rotary pump.
3. Click the [Reagent Gas] button to open the valve on the control unit.
4. Repeat Steps 2 and 3 about 5 times to extract all excess reagent gas.
5. Wait a while for the vacuum level to stabilize.
If there is still too much reagent gas introduced, repeat Steps 1 to 4 again.
If there is still too much reagent gas introduced, repeat Steps 1 to 4 again.
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