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  • No : 4689
  • Date of Issue : 2020/12/17 10:16
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(GCMS) Chemical Ionization(CI, NCI) Excessive Introduction of Reagent Gas

(GCMS) Chemical Ionization(CI, NCI) Excessive Introduction of Reagent Gas
Category : 

Answer

Sometimes too much reagent gas is introduced during reagent gas adjustment. If this happens, extract excess reagent gas by following the procedure below.
 
1. Close the pressure-regulating valve of the pressure regulator slightly.
 
 
2. Click the [Reagent Gas] button on the [Instrument Control] bar to close the valve.
  As a result, the valve of the reagent gas control unit is closed, and reagent gas in the analysis tube is extracted from the controller by the rotary pump.
 
 
 
3. Click the [Reagent Gas] button to open the valve on the control unit.
 
4. Repeat Steps 2 and 3 about 5 times to extract all excess reagent gas.
 
5. Wait a while for the vacuum level to stabilize.
  If there is still too much reagent gas introduced, repeat Steps 1 to 4 again.
  

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