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(LCMS) Setting the Peak Integration Parameters Separately for Each Compound
(LCMS) Setting the Peak Integration Parameters Separately for Each Compound
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Answer
Normally, parameter settings specified in the method for quantitative analysis are used for peak integration.
However, if there are a wide variety of peak shapes involved, that can prevent proper detection in some cases.
In such cases, appropriate parameter settings can be specified for each compound in the compound table.
HINT: This requires creating a compound table in advance. For instructions on creating a compound table, refer to “Compound Table” in the LabSolutions LCMS Instruction Manual.
1. Open the data file in the [MS Data Acquisition] window.
2. In [Method View], click [Edit] to activate the method edit mode.
3. Click the [Integration] tab.
4. Select the compound in the left pane and select the [Yes] checkbox in [Individual Setting] in the right pane.
5. Specify peak integration parameter settings for respective compounds.
6. Click [View] in [Method View] to display the method. Then save the data file by overwriting.
7. The compound table created above is registered in the data file. Save the method file by overwriting and with a separate name, so that it can be used for batch processes and for creating a calibration curve.
2. In [Method View], click [Edit] to activate the method edit mode.
3. Click the [Integration] tab.
4. Select the compound in the left pane and select the [Yes] checkbox in [Individual Setting] in the right pane.
5. Specify peak integration parameter settings for respective compounds.
6. Click [View] in [Method View] to display the method. Then save the data file by overwriting.
7. The compound table created above is registered in the data file. Save the method file by overwriting and with a separate name, so that it can be used for batch processes and for creating a calibration curve.
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