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(EDX) High-concentration "Sn" aqueous solution analysis
I wanted to analyze a high concentration aqueous Sn solution, and I created calibration curves with concentrations of 0% to 10 %. In the high concentration region, changes in intensity decreased, and the variance in quantitative values increased. Why is this?
How can I proceed with the analysis?
How can I proceed with the analysis?
Answer
When measuring high-concentration aqueous solutionswith fluorescent X-rays, the fluorescent X-ray intensity may fail to risedue to the self-absorption phenomenon, even if the content increases.
Countermeasures in this case are to dilute the aqueous solution or to change the analysis line.
Countermeasures in this case are to dilute the aqueous solution or to change the analysis line.
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