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  • No : 3297
  • Date of Issue : 2020/11/13 10:09
  • Last Updated : 2022/06/17 14:22
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Stopping the Instrument (LCMS)

Stopping the Instrument (LCMS)
Category : 

Answer

This section describes the procedure for stopping the instrument's vacuum system and up to turning the power OFF.
HINT: The vacuum status affects the instrument's sensitivity. With the exception of situations where the instrument is not used for a long time, the instrument's vacuum system should be kept on in order to maintain a high vacuum in everyday use.
    For details on daily shutdown of the instrument, click here.
 
1. Stopping the Vacuum System (LCMS-2050 is unnecessary.)
  a) Open the [System Control] window.
  b) Click [Auto Shutdown].
    If the temperature of the heated block and DL decreases below 100°C, the triple inlet turbo molecular pump and the rotary pump will stop and the inside of the vacuum housing will be opened to atmospheric pressure.
    It takes approximately 3 minutes to equalize with atmospheric pressure.
   
2. Exiting LabSolutions
  a) Turn off the operation of the LC and MS.
   
  b) Close the open window.
    Click the [File] menu and select [Exit].
   
    The [ShutDown] window is displayed.
3. Select all the items and click [OK].
    Shutdown processing will be performed.
    NOTE: Even after the interface heater has been turned OFF, the heating gas will remain ON until the interface heater cools down below the specified temperature.
    The CID gas continues to flow at 17 kPa until the valve of the CID gas cylinder is closed.
  « LCMS-2050 »
    Select [Vacuum and Power Off] in [MS] and all the items in [LC] and [PDA]. The instrument's vacuum system shuts down, and the shutdown processing is performed.
          
4. Exit LabSolutions.
    Click the [File] menu and select [Exit].
   
5. Turn off the power to each unit of the LC and MS.
6. Close the valve of the CID gas cylinder.
7. Turn off the nitrogen gas/dry air generator.
8. Mount the DL plug.

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